Information card for entry 7128655

Structure parameters

• Formula: C14 H18 O2 Si
• Calculated formula: C14 H18 O2 Si
• Title of publication: Acyl silane directed Cp*Rh(III)-catalysed alkylation/annulation reactions.
• Authors of publication: Priebbenow, Daniel L.; Hua, Carol
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 64
• Pages of publication: 7938 - 7941
• a: 6.91 ± 0.0014 Å
• b: 16.06 ± 0.003 Å
• c: 12.25 ± 0.003 Å
• α: 90°
• β: 91.67 ± 0.03°
• γ: 90°
• Cell volume: 1358.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.155
• Residual factor for significantly intense reflections: 0.1174
• Weighted residual factors for significantly intense reflections: 0.3122
• Weighted residual factors for all reflections included in the refinement: 0.3947
• Goodness-of-fit parameter for all reflections included in the refinement: 1.603
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No