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Information card for entry 7128661
Preview
Coordinates | 7128661.cif |
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Original paper (by DOI) | HTML |
Formula | C23 H19 F6 O6 P |
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Calculated formula | C23 H19 F6 O6 P |
Title of publication | The formation of cage phosphoranes and their rearrangements in the reactions of substituted 2-(3-oxo-3-phenyl)ethoxybenzo[d]-1,3,2-dioxaphospholes with perfluorodiacetyl. |
Authors of publication | Mironov, Vladimir F.; Dimukhametov, Mudaris N.; Ivkova, Gulnara A.; Khayarov, Khasan R.; Islamov, Daut R.; Litvinov, Igor A. |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2021 |
Journal volume | 57 |
Journal issue | 68 |
Pages of publication | 8516 - 8519 |
a | 10.1241 ± 0.0001 Å |
b | 13.5556 ± 0.0002 Å |
c | 34.2865 ± 0.0004 Å |
α | 90° |
β | 98.111 ± 0.001° |
γ | 90° |
Cell volume | 4658.35 ± 0.1 Å3 |
Cell temperature | 99.99 ± 0.13 K |
Ambient diffraction temperature | 99.99 ± 0.13 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | I 1 2/a 1 |
Hall space group symbol | -I 2ya |
Residual factor for all reflections | 0.0377 |
Residual factor for significantly intense reflections | 0.035 |
Weighted residual factors for significantly intense reflections | 0.091 |
Weighted residual factors for all reflections included in the refinement | 0.0928 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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