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Information card for entry 7128747
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Coordinates | 7128747.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C18 H40 Al F20 O4 P Si4 Te4 |
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Calculated formula | C18 H40 Al F20 O4 P Si4 Te4 |
Title of publication | One-step methylation of aromatic phosphorus heterocycles: synthesis and crystallographic characterization of a 1-methyl-phosphininium salt. |
Authors of publication | Fischer, Lukas; Wossidlo, Friedrich; Frost, Daniel; Coles, Nathan T.; Steinhauer, Simon; Riedel, Sebastian; Müller, Christian |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2021 |
Journal volume | 57 |
Journal issue | 75 |
Pages of publication | 9522 - 9525 |
a | 12.0027 ± 0.0004 Å |
b | 16.9978 ± 0.0005 Å |
c | 21.5539 ± 0.0007 Å |
α | 90° |
β | 90.59 ± 0.001° |
γ | 90° |
Cell volume | 4397.2 ± 0.2 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 8 |
Space group number | 9 |
Hermann-Mauguin space group symbol | C 1 c 1 |
Hall space group symbol | C -2yc |
Residual factor for all reflections | 0.018 |
Residual factor for significantly intense reflections | 0.0174 |
Weighted residual factors for significantly intense reflections | 0.0416 |
Weighted residual factors for all reflections included in the refinement | 0.0421 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.048 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7128747.html
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