Information card for entry 7128876

Structure parameters

• Formula: C24 H82 As2 N10 Na2 O91 Rh2 W22
• Calculated formula: C24 H82 As2 N10 Na2 O91 Rh2 W22
• Title of publication: A Rh-substituted polyoxometalate with an acetate-modified building block {As₂W₂₂O₇₆(CH₃COO)₂}.
• Authors of publication: Liu, Zhen; Zhang, Xue; Wan, Rong; Li, Huafeng; Hong, Yumei; Ma, Pengtao; Niu, Jingyang; Wang, Jingping
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 79
• Pages of publication: 10250 - 10253
• a: 40.0469 ± 0.0011 Å
• b: 12.2563 ± 0.0004 Å
• c: 23.2462 ± 0.0006 Å
• α: 90°
• β: 108.059 ± 0.001°
• γ: 90°
• Cell volume: 10847.8 ± 0.5 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0324
• Residual factor for significantly intense reflections: 0.0265
• Weighted residual factors for significantly intense reflections: 0.0554
• Weighted residual factors for all reflections included in the refinement: 0.0579
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No