Information card for entry 7128911

Structure parameters

• Formula: H32 K2 Ni2 O44 V10
• Calculated formula: H32 K2 Ni2 O44 V10
• Title of publication: Efficient homogeneous electrocatalytic hydrogen evolution using a Ni-containing polyoxometalate catalyst.
• Authors of publication: Jana, Debu; Kolli, Hema Kumari; Sabnam, Subhashree; Das, Samar K.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 77
• Pages of publication: 9910 - 9913
• a: 8.7397 ± 0.0004 Å
• b: 10.7629 ± 0.0005 Å
• c: 11.1283 ± 0.0005 Å
• α: 65.037 ± 0.004°
• β: 75.059 ± 0.004°
• γ: 70.54 ± 0.004°
• Cell volume: 886.32 ± 0.08 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0771
• Residual factor for significantly intense reflections: 0.0725
• Weighted residual factors for significantly intense reflections: 0.1967
• Weighted residual factors for all reflections included in the refinement: 0.2074
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No