Information card for entry 7128915

Structure parameters

• Formula: C194 H240 F18 N18 O52 Rh6 S6
• Calculated formula: C186 H182 F15 N18 O30 Rh6 S5
• Title of publication: Same knot, longer rope: altering ligand geometry provides control over nuclearity in self-assembled trefoil knots.
• Authors of publication: Wang, Qi-Li-Sha; Lin, Yue-Jian; Jin, Guo-Xin
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 76
• Pages of publication: 9772 - 9775
• a: 23.6578 ± 0.0011 Å
• b: 23.679 ± 0.0011 Å
• c: 23.8109 ± 0.0011 Å
• α: 119.776 ± 0.002°
• β: 98.285 ± 0.002°
• γ: 91.895 ± 0.002°
• Cell volume: 11371.5 ± 0.9 ų
• Cell temperature: 154 ± 2 K
• Ambient diffraction temperature: 154 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1039
• Residual factor for significantly intense reflections: 0.081
• Weighted residual factors for significantly intense reflections: 0.2032
• Weighted residual factors for all reflections included in the refinement: 0.2139
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 1.34138 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No