Information card for entry 7128926

Structure parameters

• Formula: C61.5 H44 B Cl3 F24 N3 O P Pd
• Calculated formula: C61.501 H44.002 B Cl3.002 F24 N3 O P Pd
• Title of publication: Construction of modular Pd/Cu multimetallic chains via ligand- and anion-controlled metal-metal interactions
• Authors of publication: Rivada Wheelaghan, Orestes; Deolka, Shubham; Govindarajan, Ramadoss; Khaskin, Eugene; Fayzullin, Robert R.; Pal, Shrinwantu; Khusnutdinova, Julia R.
• Journal of publication: Chemical Communications
• Year of publication: 2021
• a: 13.38647 ± 0.00013 Å
• b: 14.66903 ± 0.00016 Å
• c: 18.7357 ± 0.00019 Å
• α: 108.071 ± 0.0009°
• β: 94.0455 ± 0.0008°
• γ: 112.832 ± 0.001°
• Cell volume: 3146.07 ± 0.07 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0688
• Residual factor for significantly intense reflections: 0.0474
• Weighted residual factors for significantly intense reflections: 0.1069
• Weighted residual factors for all reflections included in the refinement: 0.1274
• Goodness-of-fit parameter for all reflections included in the refinement: 1.124
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No