Information card for entry 7128936

Structure parameters

• Formula: C32 H51 B F4 Pt4
• Calculated formula: C32 H48 B F4 Pt4
• Title of publication: Imidazolium salts and [Pt(cod)₂]: from NHC hydrido complexes to the unprecedented olefinic tetrahedral cluster [Pt₄(μ-H)(cod)₄]BF₄.
• Authors of publication: He, Fengkai; Gourlaouen, Christophe; Pang, Huan; Braunstein, Pierre
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 78
• Pages of publication: 10039 - 10042
• a: 21.3229 ± 0.0016 Å
• b: 12.7436 ± 0.0012 Å
• c: 15.3117 ± 0.0014 Å
• α: 90°
• β: 132.571 ± 0.003°
• γ: 90°
• Cell volume: 3064.1 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0908
• Residual factor for significantly intense reflections: 0.0637
• Weighted residual factors for significantly intense reflections: 0.1554
• Weighted residual factors for all reflections included in the refinement: 0.1711
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No