Information card for entry 7129357

Structure parameters

• Formula: C52 H72 B2 Cl2 Ge2 Si4
• Calculated formula: C52 H72 B2 Cl2 Ge2 Si4
• Title of publication: Borole-based half-sandwich complexes of germanium and tin
• Authors of publication: Sarcevic, Julijan; Heitkemper, Tobias; Sindlinger, Christian P.
• Journal of publication: Chemical Communications
• Year of publication: 2021
• a: 19.048 ± 0.002 Å
• b: 11.2539 ± 0.0012 Å
• c: 25.727 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5515 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0365
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0716
• Weighted residual factors for all reflections included in the refinement: 0.0756
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No