Information card for entry 7129411

Structure parameters

• Formula: C28 H104 B8 N12 Sm4
• Calculated formula: C28 H104 B8 N12 Sm4
• Title of publication: Amine–Boranes Reactions Promoted by Lanthanide(II) Ions
• Authors of publication: Kirkina, Vladislava A.; Kissel, Alexander; Selikhov, Alexander N.; Nelyubina, Yulia V.; Filippov, Oleg A.; Belkova, Natalia; Trifonov, Alexander; Shubina, Elena
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 9.7159 ± 0.0017 Å
• b: 13.065 ± 0.002 Å
• c: 13.542 ± 0.002 Å
• α: 104.319 ± 0.004°
• β: 107.514 ± 0.004°
• γ: 108.505 ± 0.003°
• Cell volume: 1438.5 ± 0.4 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1309
• Residual factor for significantly intense reflections: 0.0815
• Weighted residual factors for significantly intense reflections: 0.1839
• Weighted residual factors for all reflections included in the refinement: 0.2077
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No