Information card for entry 7129671

Structure parameters

• Formula: C21 H38 Cl Ge N Si
• Calculated formula: C21 H38 Cl Ge N Si
• Title of publication: Accessing cationic tetrylene-nickel(0) systems featuring donor-acceptor E-Ni triple bonds (E = Ge, Sn)
• Authors of publication: Hadlington, Terrance J.; Keil, Philip Maximilian
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 15.832 ± 0.003 Å
• b: 9.619 ± 0.002 Å
• c: 16.603 ± 0.003 Å
• α: 90°
• β: 112.86 ± 0.03°
• γ: 90°
• Cell volume: 2329.8 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1382
• Residual factor for significantly intense reflections: 0.0519
• Weighted residual factors for significantly intense reflections: 0.0916
• Weighted residual factors for all reflections included in the refinement: 0.1094
• Goodness-of-fit parameter for all reflections included in the refinement: 0.863
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No