Information card for entry 7129673

Structure parameters

• Formula: C42 H76 Cl3 K N2 Si2 Sn2
• Calculated formula: C42 H76 Cl3 K N2 Si2 Sn2
• Title of publication: Accessing cationic tetrylene-nickel(0) systems featuring donor-acceptor E-Ni triple bonds (E = Ge, Sn)
• Authors of publication: Hadlington, Terrance J.; Keil, Philip Maximilian
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 11.13 ± 0.002 Å
• b: 14.968 ± 0.003 Å
• c: 16.561 ± 0.003 Å
• α: 72.19 ± 0.03°
• β: 77.4 ± 0.03°
• γ: 79.94 ± 0.03°
• Cell volume: 2546.1 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0766
• Residual factor for significantly intense reflections: 0.0347
• Weighted residual factors for significantly intense reflections: 0.057
• Weighted residual factors for all reflections included in the refinement: 0.0631
• Goodness-of-fit parameter for all reflections included in the refinement: 0.883
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No