Information card for entry 7129788

Structure parameters

• Formula: C98 H98 I2 O4 Yb2
• Calculated formula: C98 H98 I2 O4 Yb2
• Title of publication: Selective carbon-phosphorus bond cleavage: expanding the toolbox for accessing bulky divalent lanthanoid sandwich complexes
• Authors of publication: Shephard, Angus; Daniels, Daisy; Deacon, Glen B.; Guo, Zhifang; Jaroschik, Florian; Junk, Peter Courtney
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 11.9588 ± 0.0002 Å
• b: 12.2903 ± 0.0001 Å
• c: 14.3366 ± 0.0001 Å
• α: 88.227 ± 0.001°
• β: 80.39 ± 0.001°
• γ: 82.417 ± 0.001°
• Cell volume: 2059.33 ± 0.04 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.036
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.0855
• Weighted residual factors for all reflections included in the refinement: 0.0868
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No