Information card for entry 7129791

Structure parameters

• Formula: C84 H66 Eu
• Calculated formula: C84 H66 Eu
• Title of publication: Selective carbon-phosphorus bond cleavage: expanding the toolbox for accessing bulky divalent lanthanoid sandwich complexes
• Authors of publication: Shephard, Angus; Daniels, Daisy; Deacon, Glen B.; Guo, Zhifang; Jaroschik, Florian; Junk, Peter Courtney
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 10.48 ± 0.002 Å
• b: 17.83 ± 0.004 Å
• c: 16.38 ± 0.003 Å
• α: 90°
• β: 94.9 ± 0.03°
• γ: 90°
• Cell volume: 3049.6 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0645
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.1387
• Weighted residual factors for all reflections included in the refinement: 0.1493
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No