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Information card for entry 7129901
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Coordinates | 7129901.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C16 H19 N O2 |
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Calculated formula | C16 H19 N O2 |
Title of publication | Extension of hydrogen borrowing alkylation reactions for the total synthesis of (−)-γ-lycorane |
Authors of publication | Hall, Christopher J. J.; Marriott, Indi S.; Christensen, Kirsten E.; Day, Aaron J.; Goundry, William R. F.; Donohoe, Timothy J. |
Journal of publication | Chemical Communications |
Year of publication | 2022 |
a | 9.5572 ± 0.0006 Å |
b | 12.2819 ± 0.001 Å |
c | 12.4294 ± 0.0006 Å |
α | 101.237 ± 0.006° |
β | 99.446 ± 0.005° |
γ | 110.609 ± 0.007° |
Cell volume | 1295.68 ± 0.17 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0839 |
Residual factor for significantly intense reflections | 0.0677 |
Weighted residual factors for all reflections | 0.2172 |
Weighted residual factors for significantly intense reflections | 0.1975 |
Weighted residual factors for all reflections included in the refinement | 0.2172 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.994 |
Diffraction radiation wavelength | 1.5418 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7129901.html
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