Information card for entry 7129918

Structure parameters

• Formula: C54 H140 Cu2 Ge18 N4 Si16
• Calculated formula: C54 H140 Cu2 Ge18 N4 Si16
• Title of publication: Oxidative Coupling of Silylated Nonagermanide Clusters
• Authors of publication: Wallach, Chistoph; Klein, Wilhelm; Fässler, Thomas F
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 16.654 ± 0.0004 Å
• b: 27.2393 ± 0.0008 Å
• c: 27.6288 ± 0.0006 Å
• α: 90°
• β: 103.416 ± 0.002°
• γ: 90°
• Cell volume: 12191.6 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/c 1
• Hall space group symbol: -I 2yc
• Residual factor for all reflections: 0.0546
• Residual factor for significantly intense reflections: 0.0311
• Weighted residual factors for significantly intense reflections: 0.0689
• Weighted residual factors for all reflections included in the refinement: 0.0818
• Goodness-of-fit parameter for all reflections included in the refinement: 1.134
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No