Information card for entry 7130017

Structure parameters

• Formula: C30 H24 F N3 O4
• Calculated formula: C30 H24 F N3 O4
• Title of publication: Catalytic asymmetric amination of azlactones with azobenzenes
• Authors of publication: Ke, Chaoqi; Cao, Qiuhui; Luo, Yao; Liu, Xiaohua; Feng, Xiaoming
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 10.3838 ± 0.0003 Å
• b: 37.4871 ± 0.001 Å
• c: 6.6582 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2591.76 ± 0.13 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0467
• Residual factor for significantly intense reflections: 0.0407
• Weighted residual factors for significantly intense reflections: 0.0987
• Weighted residual factors for all reflections included in the refinement: 0.1068
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No