Information card for entry 7130052
Formula |
C19 H12 Cl2 |
Calculated formula |
C19 H12 Cl2 |
Title of publication |
Rapid access to 9-arylfluorene and spirobifluorene through Pd-catalysed C–H arylation/deaminative annulation |
Authors of publication |
Wu, Yu; Wu, Feng-Wei; Zhou, Kun; Li, Yiming; Chen, Lei; Wang, Shuang; Xu, Zhen-Yuan; Lou, Shao-Jie; Xu, Dan-Qian |
Journal of publication |
Chemical Communications |
Year of publication |
2022 |
a |
12.013 ± 0.0014 Å |
b |
6.5987 ± 0.0007 Å |
c |
36.445 ± 0.004 Å |
α |
90° |
β |
90° |
γ |
90° |
Cell volume |
2889 ± 0.6 Å3 |
Cell temperature |
193 K |
Ambient diffraction temperature |
193 K |
Number of distinct elements |
3 |
Space group number |
61 |
Hermann-Mauguin space group symbol |
P b c a |
Hall space group symbol |
-P 2ac 2ab |
Residual factor for all reflections |
0.0672 |
Residual factor for significantly intense reflections |
0.0516 |
Weighted residual factors for significantly intense reflections |
0.1414 |
Weighted residual factors for all reflections included in the refinement |
0.1536 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.081 |
Diffraction radiation probe |
x-ray |
Diffraction radiation wavelength |
1.34139 Å |
Diffraction radiation type |
GaKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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https://www.crystallography.net/7130052.html