Information card for entry 7130084
Formula |
C15 H11 Cl N2 O |
Calculated formula |
C15 H11 Cl N2 O |
Title of publication |
TfOH-catalyzed regioselective N2-alkylation of indazoles with diazo compounds |
Authors of publication |
He, Hangli; Yan, Jingyu; Jin, Jingru; Yan, Zhewei; Yan, Qiongjiao; Wang, Wei; Jiang, Haipeng; Wang, Haifeng; Chen, Fener |
Journal of publication |
Chemical Communications |
Year of publication |
2022 |
a |
8.134 ± 0.003 Å |
b |
8.219 ± 0.003 Å |
c |
19.46 ± 0.008 Å |
α |
90° |
β |
101.5 ± 0.009° |
γ |
90° |
Cell volume |
1274.8 ± 0.8 Å3 |
Cell temperature |
296 ± 2 K |
Ambient diffraction temperature |
296 ± 2 K |
Number of distinct elements |
5 |
Space group number |
14 |
Hermann-Mauguin space group symbol |
P 1 21/c 1 |
Hall space group symbol |
-P 2ybc |
Residual factor for all reflections |
0.1031 |
Residual factor for significantly intense reflections |
0.0459 |
Weighted residual factors for significantly intense reflections |
0.0852 |
Weighted residual factors for all reflections included in the refinement |
0.1084 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.042 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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https://www.crystallography.net/7130084.html