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Information card for entry 7130155
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Coordinates | 7130155.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | ethyl 3-(8-(diphenylphosphaneyl)naphthalen-1-yl)propanoate |
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Formula | C27 H25 O2 P |
Calculated formula | C2.57143 H2.38095 O0.190476 P0.0952381 |
Title of publication | Ru(II)-catalyzed P(III)-assisted C8-alkylation of naphthphosphines |
Authors of publication | Ma, Wen-Tao; Huang, Mao-Gui; Fuyue, Liuting; Wang, Zhong-Hui; Tao, Jun-Yang; Li, Jia-Wei; Liu, Yue-Jin; Zeng, Ming-Hua |
Journal of publication | Chemical Communications |
Year of publication | 2022 |
a | 9.3822 ± 0.0003 Å |
b | 10.1224 ± 0.0004 Å |
c | 13.1212 ± 0.0004 Å |
α | 68.499 ± 0.003° |
β | 79.973 ± 0.003° |
γ | 73.741 ± 0.003° |
Cell volume | 1109.47 ± 0.07 Å3 |
Cell temperature | 100.01 ± 0.1 K |
Ambient diffraction temperature | 100.01 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0429 |
Residual factor for significantly intense reflections | 0.0401 |
Weighted residual factors for significantly intense reflections | 0.1062 |
Weighted residual factors for all reflections included in the refinement | 0.1089 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.074 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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