Information card for entry 7130184

Structure parameters

• Formula: C64 H86 Al K N2 O4 Si2
• Calculated formula: C64 H86 Al K N2 O4 Si2
• Title of publication: Diverse reactivity of an Al(I)-centred anion towards ketones.
• Authors of publication: Liu, Han-Ying; Hill, Michael S.; Mahon, Mary F.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2022
• a: 21.7511 ± 0.0004 Å
• b: 13.3392 ± 0.0002 Å
• c: 20.8348 ± 0.0003 Å
• α: 90°
• β: 101.877 ± 0.002°
• γ: 90°
• Cell volume: 5915.64 ± 0.17 ų
• Cell temperature: 150.01 ± 0.1 K
• Ambient diffraction temperature: 150.01 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0295
• Residual factor for significantly intense reflections: 0.0281
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0731
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No