Janus faced fluorocyclohexanes for supramolecular assembly: Synthesis and solid state structures of equatorial mono-, di- and tri alkylated cyclohexanes and with tri-axial C-F bonds to impart polarity.
Authors of publication
Poskin, Thomas J.; Piscelli, Bruno A.; Yoshida, Keigo; Cordes, David Bradford; Slawin, Alexandra; Cormanich, Rodrigo A.; Yamada, Shigeyuki; O'Hagan, David
Journal of publication
Chemical Communications
Year of publication
2022
a
11.7685 ± 0.0006 Å
b
4.7401 ± 0.0002 Å
c
17.0705 ± 0.001 Å
α
90°
β
103.918 ± 0.006°
γ
90°
Cell volume
924.3 ± 0.09 Å3
Cell temperature
125 K
Ambient diffraction temperature
125 K
Number of distinct elements
3
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.1147
Residual factor for significantly intense reflections
0.1045
Weighted residual factors for significantly intense reflections
0.3249
Weighted residual factors for all reflections included in the refinement
0.3408
Goodness-of-fit parameter for all reflections included in the refinement
