Janus faced fluorocyclohexanes for supramolecular assembly: Synthesis and solid state structures of equatorial mono-, di- and tri alkylated cyclohexanes and with tri-axial C-F bonds to impart polarity.
Authors of publication
Poskin, Thomas J.; Piscelli, Bruno A.; Yoshida, Keigo; Cordes, David Bradford; Slawin, Alexandra; Cormanich, Rodrigo A.; Yamada, Shigeyuki; O'Hagan, David
Journal of publication
Chemical Communications
Year of publication
2022
a
19.3963 ± 0.0011 Å
b
4.7331 ± 0.0003 Å
c
26.5239 ± 0.0015 Å
α
90°
β
95.933 ± 0.005°
γ
90°
Cell volume
2422 ± 0.2 Å3
Cell temperature
125 K
Ambient diffraction temperature
125 K
Number of distinct elements
3
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0942
Residual factor for significantly intense reflections
0.085
Weighted residual factors for significantly intense reflections
0.2468
Weighted residual factors for all reflections included in the refinement
0.2604
Goodness-of-fit parameter for all reflections included in the refinement
