Information card for entry 7130290

Structure parameters

• Formula: C44 H64 Ce2 Ge K2 O2 Si2
• Calculated formula: C44 H64 Ce2 Ge K2 O2 Si2
• Title of publication: Silole and germole complexes of lanthanum and cerium
• Authors of publication: Sun, Xiaofei; Münzfeld, Luca; Jin, Da; Hauser, Adrian; Roesky, Peter W.
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 12.9801 ± 0.0007 Å
• b: 23.8817 ± 0.0016 Å
• c: 31.57 ± 0.003 Å
• α: 90°
• β: 96.258 ± 0.006°
• γ: 90°
• Cell volume: 9728 ± 1.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0405
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.0766
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No