Information card for entry 7130316

Structure parameters

• Formula: C23 H20 N2 O
• Calculated formula: C23 H20 N2 O
• Title of publication: Substrate-directed divergent synthesis of fused indole polycycles through Rh(II)-catalyzed cascade reactions of bis(diazo)indolin-2-ones
• Authors of publication: Zhao, Yang; Niu, Xin-Yue; Yang, Hong; Yang, Jing; Wang, Zhizeng; Wang, Qi-Lin
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 9.674 ± 0.003 Å
• b: 9.935 ± 0.003 Å
• c: 10.704 ± 0.003 Å
• α: 87.411 ± 0.011°
• β: 65.196 ± 0.011°
• γ: 76.494 ± 0.012°
• Cell volume: 906.4 ± 0.5 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273.15 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1068
• Residual factor for significantly intense reflections: 0.0814
• Weighted residual factors for significantly intense reflections: 0.2359
• Weighted residual factors for all reflections included in the refinement: 0.268
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No