Crystallography Open Database

Information card for entry 7130338

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Coordinates	7130338.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C234 H252 N24 O60 Rh12
Calculated formula	C234 H252 N24 O60 Rh12
Title of publication	Synthesis of the Two Isomers of Heteroleptic Rh12L6L’6 Metal-Organic Polyhedra by Screening of Complementary Linkers
Authors of publication	Broto-Ribas, Anna; Gutiérrez, Susana; Imaz, Inhar; Carné-Sánchez, Arnau; Gándara, Felipe; Juanhuix, Judith; Maspoch, Daniel
Journal of publication	Chemical Communications
Year of publication	2022
a	33.9017 ± 0.0002 Å
b	33.9017 ± 0.0002 Å
c	23.6843 ± 0.0007 Å
α	90°
β	90°
γ	120°
Cell volume	23574 ± 0.7 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.1094
Residual factor for significantly intense reflections	0.0806
Weighted residual factors for significantly intense reflections	0.2342
Weighted residual factors for all reflections included in the refinement	0.2602
Goodness-of-fit parameter for all reflections included in the refinement	0.985
Diffraction radiation wavelength	0.82656 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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