Information card for entry 7130341

Structure parameters

• Formula: C252 H252 N6 O72 Rh12
• Calculated formula: C252 H252 N6 O72 Rh12
• Title of publication: Synthesis of the Two Isomers of Heteroleptic Rh12L6L’6 Metal-Organic Polyhedra by Screening of Complementary Linkers
• Authors of publication: Broto-Ribas, Anna; Gutiérrez, Susana; Imaz, Inhar; Carné-Sánchez, Arnau; Gándara, Felipe; Juanhuix, Judith; Maspoch, Daniel
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 31.6843 ± 0.0005 Å
• b: 31.6843 ± 0.0005 Å
• c: 72.349 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 62900 ± 2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 167
• Hermann-Mauguin space group symbol: R -3 c :H
• Hall space group symbol: -R 3 2"c
• Residual factor for all reflections: 0.1354
• Residual factor for significantly intense reflections: 0.1105
• Weighted residual factors for significantly intense reflections: 0.3237
• Weighted residual factors for all reflections included in the refinement: 0.3509
• Goodness-of-fit parameter for all reflections included in the refinement: 1.245
• Diffraction radiation wavelength: 0.82656 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No