Information card for entry 7130354

Structure parameters

• Formula: C20 H27 Ge N O5 Si W
• Calculated formula: C20 H27 Ge N O5 Si W
• Title of publication: Heavier N-heterocyclic half-sandwich tetrylenes
• Authors of publication: Bischoff, Inga-Alexandra; Morgenstern, Bernd; Schäfer, André
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 9.1997 ± 0.0004 Å
• b: 26.2141 ± 0.001 Å
• c: 10.2037 ± 0.0004 Å
• α: 90°
• β: 100.75 ± 0.002°
• γ: 90°
• Cell volume: 2417.56 ± 0.17 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0299
• Residual factor for significantly intense reflections: 0.022
• Weighted residual factors for significantly intense reflections: 0.0426
• Weighted residual factors for all reflections included in the refinement: 0.0453
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No