Information card for entry 7130356

Structure parameters

• Formula: C26 H47 N3 Pb Si
• Calculated formula: C26 H47 N3 Pb Si
• Title of publication: Heavier N-heterocyclic half-sandwich tetrylenes
• Authors of publication: Bischoff, Inga-Alexandra; Morgenstern, Bernd; Schäfer, André
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 9.0843 ± 0.0002 Å
• b: 15.3056 ± 0.0004 Å
• c: 10.2605 ± 0.0003 Å
• α: 90°
• β: 98.369 ± 0.001°
• γ: 90°
• Cell volume: 1411.43 ± 0.06 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0147
• Residual factor for significantly intense reflections: 0.0134
• Weighted residual factors for significantly intense reflections: 0.029
• Weighted residual factors for all reflections included in the refinement: 0.0292
• Goodness-of-fit parameter for all reflections included in the refinement: 0.868
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No