Information card for entry 7130430

Structure parameters

• Formula: C398 H542 Ag50 F36 N18 O74 S32 V10
• Calculated formula: C360 H472 Ag50 F24 N8 O56 S32 V10
• Title of publication: A classical [V10O28]6− anion templated high-nuclearity silver thiolate cluster
• Authors of publication: Li, Li; Zhu, Yanjie; Han, Baoliang; Wang, Qiongyi; Zheng, Luming; Feng, Lei; Sun, Di; Wang, Zhi
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 25.6844 ± 0.0003 Å
• b: 27.1429 ± 0.0002 Å
• c: 36.546 ± 0.0004 Å
• α: 90°
• β: 91.7718 ± 0.0009°
• γ: 90°
• Cell volume: 25465.8 ± 0.4 ų
• Cell temperature: 99.9 ± 0.3 K
• Ambient diffraction temperature: 99.9 ± 0.3 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1575
• Residual factor for significantly intense reflections: 0.1448
• Weighted residual factors for significantly intense reflections: 0.3506
• Weighted residual factors for all reflections included in the refinement: 0.3593
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No