Information card for entry 7130459

Structure parameters

• Formula: C42 H92 As2 O6
• Calculated formula: C42 H92 As2 O6
• Title of publication: A surprise landing on the <i>terra incognita</i> of macrocyclic dibridgehead diorganoarsines: syntheses, structures, and reactivities.
• Authors of publication: Zarcone, Samuel R.; Verardi, Peter J.; Bhuvanesh, Nattamai; Gladysz, John A.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2022
• Journal volume: 58
• Journal issue: 62
• Pages of publication: 8694 - 8697
• a: 8.6319 ± 0.0006 Å
• b: 13.4245 ± 0.001 Å
• c: 20.7781 ± 0.0015 Å
• α: 72.297 ± 0.002°
• β: 84.548 ± 0.002°
• γ: 88.073 ± 0.002°
• Cell volume: 2283.3 ± 0.3 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0717
• Residual factor for significantly intense reflections: 0.0678
• Weighted residual factors for significantly intense reflections: 0.1677
• Weighted residual factors for all reflections included in the refinement: 0.1707
• Goodness-of-fit parameter for all reflections included in the refinement: 1.169
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No