Information card for entry 7130491

Structure parameters

• Formula: C47.5 H71 Cl Ga N3 Si Sn
• Calculated formula: C47.5 H71 Cl Ga N3 Si Sn
• Title of publication: Structurally characterised intermediate of the oxidative addition of a heteroleptic germylene to gallanediyle
• Authors of publication: Bücker, Anna; Wölper, Christoph; Haberhauer, Gebhard; Schulz, Stephan
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 21.6428 ± 0.0013 Å
• b: 11.8899 ± 0.0008 Å
• c: 19.3967 ± 0.0011 Å
• α: 90°
• β: 107.608 ± 0.003°
• γ: 90°
• Cell volume: 4757.5 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.0707
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1334
• Weighted residual factors for all reflections included in the refinement: 0.1564
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No