Information card for entry 7130497

Structure parameters

• Formula: C73.5 H69.75 Al F36.75 Ga Ge N2 O4
• Calculated formula: C72 H68.5 Al F36.5 Ga Ge N2 O4
• Title of publication: Structurally characterised intermediate of the oxidative addition of a heteroleptic germylene to gallanediyle
• Authors of publication: Bücker, Anna; Wölper, Christoph; Haberhauer, Gebhard; Schulz, Stephan
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 25.1362 ± 0.0016 Å
• b: 17.414 ± 0.0011 Å
• c: 36.805 ± 0.002 Å
• α: 90°
• β: 96.472 ± 0.002°
• γ: 90°
• Cell volume: 16007.7 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0514
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.1227
• Weighted residual factors for all reflections included in the refinement: 0.1262
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No