Information card for entry 7130511

Structure parameters

• Formula: C39 H55 B2 N12 P U
• Calculated formula: C39 H55 B2 N12 P U
• Title of publication: Isolation of uranium(iii) primary phosphido complexes
• Authors of publication: Perales, Diana; Bhowmick, Rina; Zeller, Matthias; Miro, Pere; Vlaisavljevich, Bess; Bart, Suzanne C.
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 10.9713 ± 0.0008 Å
• b: 11.9909 ± 0.0011 Å
• c: 17.0052 ± 0.0012 Å
• α: 78.759 ± 0.005°
• β: 75.724 ± 0.004°
• γ: 86.939 ± 0.005°
• Cell volume: 2126.4 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0911
• Residual factor for significantly intense reflections: 0.0645
• Weighted residual factors for significantly intense reflections: 0.176
• Weighted residual factors for all reflections included in the refinement: 0.1945
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No