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Information card for entry 7130603
Preview
Coordinates | 7130603.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H24 N2 O4 |
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Calculated formula | C27 H24 N2 O4 |
Title of publication | Cascade reaction of o-enoyl arylisocyanide and o-hydroxy aromatic aldimine: a diastereoselective access to polycyclic spirobenzoxazine chromeno[4,3-b]pyrrole derivative |
Authors of publication | Li, Jian; Xiao, Yao; Peng, Xin; Shen, Jie; Cui, Lei; Lu, Shanya; Jia, Xueshun; Li, Chunju |
Journal of publication | Chemical Communications |
Year of publication | 2022 |
a | 11.35547 ± 0.00013 Å |
b | 16.3842 ± 0.00016 Å |
c | 12.90723 ± 0.00015 Å |
α | 90° |
β | 113.063 ± 0.0014° |
γ | 90° |
Cell volume | 2209.46 ± 0.05 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0395 |
Residual factor for significantly intense reflections | 0.0364 |
Weighted residual factors for significantly intense reflections | 0.0921 |
Weighted residual factors for all reflections included in the refinement | 0.0943 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7130603.html
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Users of the data should acknowledge the original authors of the
structural data.