Information card for entry 7130674

Structure parameters

• Formula: C47 H33 Al Cl2 F36 N O5 Sb
• Calculated formula: C47 H33 Al Cl2 F36 N O5 Sb
• Title of publication: Crystallographic evidence for a continuum and reversal of roles in primary-secondary interactions in antimony Lewis acids: applications in carbonyl activation.
• Authors of publication: Sharma, Deepti; Benny, Annabel; Gupta, Radhika; Jemmis, Eluvathingal D.; Venugopal, Ajay
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2022
• Journal volume: 58
• Journal issue: 78
• Pages of publication: 11009 - 11012
• a: 12.3903 ± 0.0018 Å
• b: 15.266 ± 0.002 Å
• c: 17.646 ± 0.003 Å
• α: 99.484 ± 0.005°
• β: 109.81 ± 0.005°
• γ: 106.208 ± 0.004°
• Cell volume: 2888.5 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0809
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for significantly intense reflections: 0.1135
• Weighted residual factors for all reflections included in the refinement: 0.1319
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No