Information card for entry 7130676

Structure parameters

• Formula: C47 H33 Al F36 N O5 Sb
• Calculated formula: C47 H33 Al F36 N O5 Sb
• Title of publication: Crystallographic evidence for a continuum and reversal of roles in primary-secondary interactions in antimony Lewis acids: applications in carbonyl activation.
• Authors of publication: Sharma, Deepti; Benny, Annabel; Gupta, Radhika; Jemmis, Eluvathingal D.; Venugopal, Ajay
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2022
• Journal volume: 58
• Journal issue: 78
• Pages of publication: 11009 - 11012
• a: 13.7542 ± 0.0011 Å
• b: 14.4647 ± 0.0012 Å
• c: 15.6531 ± 0.0013 Å
• α: 97.575 ± 0.003°
• β: 112.199 ± 0.002°
• γ: 98.467 ± 0.003°
• Cell volume: 2791.5 ± 0.4 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0397
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0693
• Weighted residual factors for all reflections included in the refinement: 0.0747
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No