Information card for entry 7130716

Structure parameters

• Formula: C132 H206 N13 Na7 O110 P14 V18 W4
• Calculated formula: C92 H66 Na7 O96 P14 V18 W4
• Title of publication: High-nuclear polyoxovanadates assembled from pentagonal building blocks
• Authors of publication: Zhang, Ting; Hou, Yuhan; Hou, Baoshan; Zhao, Liang; Wang, Xinlong; Qin, Chao; Su, Zhongmin
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 37.4678 ± 0.0017 Å
• b: 28.5413 ± 0.001 Å
• c: 20.4155 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 21831.9 ± 1.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173.02 K
• Number of distinct elements: 8
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.1405
• Residual factor for significantly intense reflections: 0.0988
• Weighted residual factors for significantly intense reflections: 0.2526
• Weighted residual factors for all reflections included in the refinement: 0.2844
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No