Information card for entry 7130803

Structure parameters

• Formula: C26 H49 N6 P Si
• Calculated formula: C26 H49 N6 P Si
• Title of publication: Crystalline phosphino(silyl)carbenes that readily form transition metal complexes
• Authors of publication: Löwe, Pawel; Dielmann, Fabian
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 10.471 ± 0.0002 Å
• b: 11.9664 ± 0.0003 Å
• c: 12.7029 ± 0.0003 Å
• α: 79.355 ± 0.001°
• β: 73.785 ± 0.001°
• γ: 74.405 ± 0.001°
• Cell volume: 1461.71 ± 0.06 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0616
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.1129
• Weighted residual factors for all reflections included in the refinement: 0.1216
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No