Information card for entry 7130808

Structure parameters

• Formula: C40 H73 Cu2 N6 O2 P Si
• Calculated formula: C40 H73 Cu2 N6 O2 P Si
• Title of publication: Crystalline phosphino(silyl)carbenes that readily form transition metal complexes
• Authors of publication: Löwe, Pawel; Dielmann, Fabian
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 21.6481 ± 0.0009 Å
• b: 18.7415 ± 0.0008 Å
• c: 22.4951 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9126.7 ± 0.7 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0672
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1432
• Weighted residual factors for all reflections included in the refinement: 0.1538
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No