Information card for entry 7130864

Structure parameters

• Formula: C26 H29 B O2 Si
• Calculated formula: C26 H29 B1.00168 O2 Si
• Title of publication: Directed <i>cis</i>-hydrosilylation of borylalkynes to borylsilylalkenes.
• Authors of publication: Stefanowska, Kinga; Sokolnicki, Tomasz; Walkowiak, Jędrzej; Czapik, Agnieszka; Franczyk, Adrian
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2022
• Journal volume: 58
• Journal issue: 86
• Pages of publication: 12046 - 12049
• a: 19.7542 ± 0.0004 Å
• b: 20.3725 ± 0.0003 Å
• c: 21.9182 ± 0.0005 Å
• α: 96.7187 ± 0.0014°
• β: 112.361 ± 0.0019°
• γ: 114.97 ± 0.0017°
• Cell volume: 6977.9 ± 0.3 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0564
• Residual factor for significantly intense reflections: 0.0436
• Weighted residual factors for significantly intense reflections: 0.1296
• Weighted residual factors for all reflections included in the refinement: 0.143
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No