Information card for entry 7130960

Structure parameters

• Formula: C100 H64 Al4 Cl8 O8 P4
• Calculated formula: C100 H64 Al4 Cl8 O8 P4
• Title of publication: A strained intramolecular P/Al-FLP and its reactivity toward allene
• Authors of publication: Federmann, Patrick; Bosse, Tamino; Wolff, Siad; Cula, Beatrice; Herwig, Christian; Limberg, Christian
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 12.083 ± 0.003 Å
• b: 13.097 ± 0.003 Å
• c: 13.743 ± 0.003 Å
• α: 88.302 ± 0.007°
• β: 86.483 ± 0.008°
• γ: 87.468 ± 0.008°
• Cell volume: 2167.8 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0709
• Residual factor for significantly intense reflections: 0.0483
• Weighted residual factors for significantly intense reflections: 0.1029
• Weighted residual factors for all reflections included in the refinement: 0.1148
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No