Information card for entry 7130962

Structure parameters

• Formula: C27 H25 P Sn
• Calculated formula: C27 H25 P Sn
• Title of publication: A strained intramolecular P/Al-FLP and its reactivity toward allene
• Authors of publication: Federmann, Patrick; Bosse, Tamino; Wolff, Siad; Cula, Beatrice; Herwig, Christian; Limberg, Christian
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 9.8677 ± 0.0004 Å
• b: 12.9432 ± 0.0005 Å
• c: 18.0733 ± 0.0008 Å
• α: 90°
• β: 94.123 ± 0.002°
• γ: 90°
• Cell volume: 2302.34 ± 0.16 ų
• Cell temperature: 102 ± 2 K
• Ambient diffraction temperature: 102 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.019
• Residual factor for significantly intense reflections: 0.0185
• Weighted residual factors for significantly intense reflections: 0.0451
• Weighted residual factors for all reflections included in the refinement: 0.0453
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No