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Information card for entry 7131106
Preview
Coordinates | 7131106.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H29 B10 N |
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Calculated formula | C23 H29 B10 N |
Title of publication | Iridium-catalyzed regioselective B(3,6)-dialkenylation or B(4)-alkenylation of <i>o</i>-carboranes <i>via</i> B-H activation and 1,2-carbon migration of alkynes. |
Authors of publication | Zhang, Huifang; Cheng, Ruofei; Qiu, Zaozao; Xie, Zuowei |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2023 |
Journal volume | 59 |
Journal issue | 6 |
Pages of publication | 740 - 743 |
a | 8.1724 ± 0.0006 Å |
b | 11.9352 ± 0.001 Å |
c | 13.5589 ± 0.001 Å |
α | 108.242 ± 0.005° |
β | 94.126 ± 0.005° |
γ | 99.211 ± 0.005° |
Cell volume | 1229.31 ± 0.17 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0804 |
Residual factor for significantly intense reflections | 0.0636 |
Weighted residual factors for significantly intense reflections | 0.1661 |
Weighted residual factors for all reflections included in the refinement | 0.1817 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.072 |
Diffraction radiation wavelength | 1.34139 Å |
Diffraction radiation type | GaKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7131106.html
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