Information card for entry 7131124

Structure parameters

• Formula: C15 H2 B Cl3 F10 N O2
• Calculated formula: C15 H2 B Cl3 F10 N O2
• Title of publication: Transient hydroboration and hydroalumination of activated azo-species: avenues to NBO and NAlO-heterobicycles.
• Authors of publication: Mandal, Dipendu; Hussain, Zahid; Luo, Yong-An; Wu, Yile; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 6
• Pages of publication: 780 - 783
• a: 10.4303 ± 0.0011 Å
• b: 15.7714 ± 0.0015 Å
• c: 11.0532 ± 0.0009 Å
• α: 90°
• β: 102.294 ± 0.006°
• γ: 90°
• Cell volume: 1776.6 ± 0.3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0883
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1104
• Weighted residual factors for all reflections included in the refinement: 0.131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No