Information card for entry 7131257

Structure parameters

• Formula: C57 H64 B4 Eu2 N24
• Calculated formula: C57 H56 B4 Eu2 N24
• Title of publication: Reduction chemistry yields stable and soluble divalent lanthanide tris(pyrazolyl)borate complexes.
• Authors of publication: Chowdhury, Tajrian; Evans, Matthew J.; Coles, Martyn P.; Bailey, Anna G.; Peveler, William J.; Wilson, Claire; Farnaby, Joy H.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 15
• Pages of publication: 2134 - 2137
• a: 10.8751 ± 0.0004 Å
• b: 12.1292 ± 0.0005 Å
• c: 13.2669 ± 0.0004 Å
• α: 81.942 ± 0.001°
• β: 68.671 ± 0.001°
• γ: 73.751 ± 0.001°
• Cell volume: 1563.57 ± 0.1 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0389
• Weighted residual factors for significantly intense reflections: 0.0826
• Weighted residual factors for all reflections included in the refinement: 0.0863
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No