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Information card for entry 7131261
Preview
Coordinates | 7131261.cif |
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Original paper (by DOI) | HTML |
Formula | C26.5 H40 B2 F1.5 K0.5 N12 O5.5 S0.5 Yb |
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Calculated formula | C26.5 H40 B2 F1.5 K0.5 N12 O5.5 S0.5 Yb |
Title of publication | Reduction chemistry yields stable and soluble divalent lanthanide tris(pyrazolyl)borate complexes. |
Authors of publication | Chowdhury, Tajrian; Evans, Matthew J.; Coles, Martyn P.; Bailey, Anna G.; Peveler, William J.; Wilson, Claire; Farnaby, Joy H. |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2023 |
Journal volume | 59 |
Journal issue | 15 |
Pages of publication | 2134 - 2137 |
a | 11.4074 ± 0.0006 Å |
b | 11.9061 ± 0.0006 Å |
c | 27.7046 ± 0.0015 Å |
α | 90.55 ± 0.002° |
β | 95.543 ± 0.002° |
γ | 99.885 ± 0.002° |
Cell volume | 3688.3 ± 0.3 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 9 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0362 |
Residual factor for significantly intense reflections | 0.0332 |
Weighted residual factors for significantly intense reflections | 0.079 |
Weighted residual factors for all reflections included in the refinement | 0.0803 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.121 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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