Information card for entry 7131282

Structure parameters

• Formula: C32 H37 Co N2 O3.187
• Calculated formula: C32 H37 Co N2 O3.187
• Title of publication: C-H bond activations by the HO˙/(Salophen^<i>t</i>-Bu)Co(II) radical pair generated <i>via</i> homolysis of a terminal Co(III)-OH bond.
• Authors of publication: Zhang, Jia; Li, Songyi; Fang, Huayi
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 22
• Pages of publication: 3245 - 3248
• a: 8.833 ± 0.0002 Å
• b: 12.9871 ± 0.0004 Å
• c: 13.374 ± 0.0004 Å
• α: 79.77 ± 0.002°
• β: 73.532 ± 0.002°
• γ: 71.813 ± 0.002°
• Cell volume: 1391.06 ± 0.07 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0428
• Residual factor for significantly intense reflections: 0.0408
• Weighted residual factors for significantly intense reflections: 0.1239
• Weighted residual factors for all reflections included in the refinement: 0.1255
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0375
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No