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Information card for entry 7131389
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Coordinates | 7131389.cif |
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Original paper (by DOI) | HTML |
Formula | C21 H23 N O4 S |
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Calculated formula | C21 H23 N O4 S |
Title of publication | Construction of oxygenated 2-azabicyclo[2.2.1]heptanes <i>via</i> palladium-catalyzed 1,2-aminoacyloxylation of cyclopentenes. |
Authors of publication | Zhou, Haipin; Pan, Rui; Xu, Menghua; Ma, Jiao; Lin, Aijun; Yao, Hequan |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2023 |
Journal volume | 59 |
Journal issue | 24 |
Pages of publication | 3574 - 3577 |
a | 16.6782 ± 0.0006 Å |
b | 8.0492 ± 0.0003 Å |
c | 14.5029 ± 0.0005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1946.96 ± 0.12 Å3 |
Cell temperature | 170 K |
Ambient diffraction temperature | 170 K |
Number of distinct elements | 5 |
Space group number | 29 |
Hermann-Mauguin space group symbol | P c a 21 |
Hall space group symbol | P 2c -2ac |
Residual factor for all reflections | 0.0487 |
Residual factor for significantly intense reflections | 0.0355 |
Weighted residual factors for significantly intense reflections | 0.0737 |
Weighted residual factors for all reflections included in the refinement | 0.0818 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.088 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7131389.html
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