Information card for entry 7131408

Structure parameters

• Formula: C133 H108 Cl2 F24 N4 O2 Os2 P6 Sb4
• Calculated formula: C133 H108 Cl2 F24 N4 O2 Os2 P6 Sb4
• Title of publication: Hetero-carbolong chemistry: experimental and theoretical studies of diaza-metallapentalenes.
• Authors of publication: Chu, Zhenwei; Li, Jinhua; Hua, Yuhui; Luo, Ming; Chen, Dafa; Xia, Haiping
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 28
• Pages of publication: 4173 - 4176
• a: 11.6995 ± 0.0009 Å
• b: 21.8835 ± 0.0015 Å
• c: 25.5349 ± 0.0019 Å
• α: 104.879 ± 0.004°
• β: 91.321 ± 0.004°
• γ: 95.31 ± 0.004°
• Cell volume: 6283.8 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0749
• Residual factor for significantly intense reflections: 0.0539
• Weighted residual factors for significantly intense reflections: 0.1341
• Weighted residual factors for all reflections included in the refinement: 0.1448
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No